/sci/ - Science & Math

>Chinesium lab equipment saves the day

It's over

>>15645085
it never even began

>>15645066
lmfao roflcopter xD

>>15645066
Yeah right I'm totally sure that's the case

>>15645066
>twitter
nah bro i don't believe you anymore

>>15645066
So you just need oxygen and it works? So what's the problem?

>>15645066
You're wrong, it was a cosmic ray that went through the sample at the perfectly right direction at the right time

it's OVER you niggers

>>15645209
If it's that simple all you need to do it point a electron beam at the sample
Has anyone tried that yet?

>>15645218
unfortunately, the person doing the experiment must ALSO have eaten chocolate ice cream about 1.5 hours before, as the metabolites produced in its digestion will adsorb on the sample and lower the energy barrier for reaching the superconductive state

this was obvious but too long to write in the preprint

>>15645066
Back bros, the needle just moved in our direction.

>>15645066
We're back

>>15645066
Or they used the other (II,IV) oxide, which has more oxygen than the stated lead (II) oxide.

>>15645230
>>15645233
Always has been
Overfags have just been coping all along

>>15645230
Never left. Oversissies want you out.

>>15645066
>another tranime material scientist

>>15645299
>another
Isn't this THE anime material scientist?

>>15645132
What's Twitter?

>>15645066
Just give China the Nobel Prize already. The fucking Koreans can't do anything right, and nobody was able to replicate it successfully until the Chinese scientists figured out the RIGHT away.

>You need to bake it in a vacuum
>NO! YOU NEED OXYGEN!

maybe cooling process needs to have atmospheric pressure (or maybe higher?) in the last part of the process to put pressure on the sponge inside. maybe use inert gas

>>15645066
Wow! just how convenient!!! I'm sure they will finally be able to replicate this ambient temperature superconductor! just 2 more weeks! Thank you Dr. Tranny and the science team at Gweilo Sum Fuk

>>15645066
>You have to grind up lead, copper, and Brimstone in a mortar and pestle
>Bake it in a furnace
>quench it to room temperature
Alchemy bros...

>>15645066
The absolute state of chinese science

>>15645066
Even der Fuhrer accepts the material has something odd about it

>>15645066
> turns out you need to heat it in a normal atmosphere
> turns out you need to use baking soda instead of lead
> turns out you need to powderize coca leaves

Uh... we're making crack, right?

>>15645066
>yet more manic "here's how we can still win!!!" twatter troon accounts
thread hidden

>>15645299
Unfortunately autism is highly correlated between being a furry, a tranny and being a successful programmer or scientist due to it giving you the ability to laser focus on a task.

>>15646498
fuck off anime troon
ywnbaj

>>15646515
you will never be a jew either but I'm completely happy being a straight white male

>>15646515
>he hasn't seen just how many hardware hackers, speed runners, etc are autistic trannies or furries
autism gives you the ability to focus and persevere on shit to the point of insanity but comes with the inability to recognize social cues as well as other idiocy

>>15645066
didn't we know already that the tube needed to be broken to let oxygen in?

>>15646534
>autism
ypu're a low functioning subhuman, even negros mog you

>>15645299
>>15645303
>>15646483
>>15646515

tfw even 4chan dwellers can’t tell the difference between two different anime pfp accounts

>>15646539
tranime niggers out
>inb4 tranime website
negrom00t left, sorry

>>15646545
>tranime
back to /leftypol/

>>15646559
>/leftypol/ even tho last time i visited them, they banned basedjaks and pepes and you have mod mandated tranime reaction pic

>>15646539
the funny thing is these two accounts are actually the only beefing accounts in all of LK99 twitter, the guy in the OP thinks that the russian guy is a fake and a fraud with a hoax replication attempt

>>15646589
The guy in the op is right then

>>15646589
Slutbaggranniesuka

Lick my barken booper

>>15646539
She's cute. Where's she from?

>>15646629
Transylvania

>>15646651
Sounds like a cool anime. I'll check it out.

They are gonna bury all the story aren't they

I think the nature of the game requires to try but not possible. only maybe delay shit a bit. even few days may be an advantage depending on situation.

>>15645191
Do we not even need the vacuum pump anymore?
Shit, anyone with a kiln could make this.
Maybe strict temperature control isn't even all that necessary.
Imagine tweakers making this from car batteries, match heads and stolen copper.
Could probably sell it on eBay before the science soibois even get their grant proposals written.

>>15646974

I honestly wouldn't even be surprised if it suddenly turned out that this is piss easy to make and it also exists in nature.
And who knows how much of this compound gets dumped into a landfill as a waste product from industries.
No one has just bothered to look because the compounds are so damn simple.

>>15646999
Here are the instructions. If you have $500 dollars and a couple of neurons you can do it.

Step 1 - Preparation for lanarkite, Pb2SO
>PbO and PbSO4 powders were uniformly mixed in a molar ratio of 1:1 in an agate mortar with a pestle. And then, after the sample was transferred to an alumina crucible, it was reacted at 725 °C for 24 hour in a furnace. After completion of the reaction, white sample was obtained. It was pulverized with the mortar.

Step 2 - Preparation for copper phosphide, Cu3P
>Cu and P powders were mixed in each composition ratio. And the sample was transferred in a quartz tube. The tube was sealed and reacted at 550 °C for 48 hour in a furnace. After taken out from the tube, a dark gray ingot was obtained and pulverized.

Step 3 - Sample Synthesis and Preparation of LK-99
>For the sample synthesis of the LK-99, the general solid-state reaction was used. Lanarkite and Cu3P were uniformly mixed in a molar ratio of 1:1 in an agate mortar with a pestle. The sample was put into a reaction tube and reacted at 925°C for 10 hr. After the reaction, a dark gray ingot was obtained reproducibly and then made into the shape of thin cuboids for electrical measurements. For other analyses, it was pulverized and used as the form of powder. The reagents used for the above solid- state reaction was PbO (JUNSEI, GR), PbSO4 (KANTO, GR), Cu (DAEJUNG, EP), and P (JUNSEI, EP).

>>15647082
Should the tube not be pressurized with oxygen or ozone as per recent suggestions?

>>15647104
I’m not sure yet. I have acquired everything necessary and will start experimentation tomorrow. I will try different methods and verify results. If anyone wants to join and do this together I can start a thread tomorrow and we can try to help one another get through this.

>>15645066
Anime avatar, what a fucking giant faggot. Hope he winds up stuck in a lorry axel.

>>15646675
Faggot kill yourself in a fire.

>>15647194
>ozempic shill
>whats that? *search*
>medicine to lose weight for massively fat fucks
>mfw

>>15647175
I cannot partake in experimentation, but I would love to follow along if you make a thread

>>15645226
>Mfw I ate chocolate ice cream and I’m now a super conductor
I’m back boys

>>15647287
I think you meant
>a sugar conductor

>>15646545
anime website

>>15645066
Since LK-99 seems easy to make without advanced equipment, this is probably how the ancient people moved all those huge stones around.

>>15647317
It is no longer an anime website, there are only anime boards.
Anime-fags are fags

>>15647082
If it needs vacuum, cheap solutions will land you at ~$1000 for the equipment to make LK99. If you don't need vacuum in the last step, which is contrary to the paper's recipe but suggested, you can knock off the vacuum equipment and it'll be only ~$500.

>>15647349
you are underaged

>>15647175
I'm keen

>>15647432
>>15647368
>>15647255
Tomorrow we start. I will make a thread. Hope to see you all.

>>15646974
>>15646999
Is it possible LK99-likes have always existed in nature and that any of the ancient unga bungas who discovered it just assumed it was regular magnetism from magnetite or some other shit impurity?

>>15647482
There are unga bungas ITT who still assume that

>>15647343
Now we need to how the hell they cut them with 90 degree angles without power tools.

And last the mistery of the incan ruins like machu picchu, the rocks look like they were soft and then were hardened in place.

>>15647482
maybe in out space in some particular conditions. maybe. so some sort of meteorite? but low chances of high purity because of random conditions, and could easily be mistaken for some magnet rock or something. especially if the magnetic effect is low.
ancient humans were retarded because they lacked information. I don't care about your fantasies.

>>15646974
>psst, hey kid want some grams of rtsc

>>15645299
>>15646545
>tranime
Ok gaslighting tranny

>>15647175
>>15647471
use a tripcode. i have a background in chemistry which could help.
in the meantime skim through how nilered oxygenated his YBCO sample.
we will make /sci/ great again

>>15647343
>>15647482
If it formed in nature we probably would have found it by now. We didn't. Pic related.

Maybe the Ancients could have made it from lead, gold, human bones and maybe sulfur if a certain Chinese paper is to be believed. All of alchemical / occult significance.

/X/ has been dumping papers about how a superconducting discharge tube creates some kind of scalar or gravitational wave. Piss easy to make if true.

But it's probably bullshit.
Ancients probably would have needed inspiration from the Archons if not bullshit.
Probably worth trying to meme it into reality anyway.
Only way we'll get off this rock before Globohomo de-evolves us is if we meme that someone already left.

>>15647525
>/X/ has been dumping papers about how a superconducting discharge tube creates some kind of scalar or gravitational wave. Piss easy to make if true.
Is that on their board now? Sounds like an entertaining claim

>>15647471
Looking forward to it

I don't know, probably, it was there two days ago.
Maybe some sorcerer needs to smoke a whole bunch of toad juice and go back in time and give them the formula.

>>15647471
don't be afraid to post all your hiccups and failures. you don't have to impress when anonymous. we'll be morons together, fren. /sci/ will figure it out

Here you go:
Whole thread is great.
>>>/x/35487394

Save the thread and any papers you want now before globohomo realizes 4chins is looking into this.
Currently snarfing up the researchgate papers

>A totally different view of the whole process is offered by the universons model. In that model,
the background universons flux enters the local and total balance of energy and momentum and can
completely alter it. For comparison, according to the virtual gravitons model there is in the emitter
an exchange of momentum with the vacuum, but not an exchange of energy; and the propagation
of the radiation and its interaction with the targets do not involve any further interaction with the
vacuum.

>Our theoretical simulation of the electromagnetic recoil of a Josephson junction suggests that
that kind of recoil is much smaller than the one observed. More realistic simulations should take
into account the penetration of strong pulsed electric fields into the insulating layers between the
YBCO grains, and effects at the YBCO-metal junctions. This appears to be out of reach of the
standard superconductivity theory, and will require further investigation.

>Independently from the theoretical interpretations, the possible practical applications of both
the anomalous radiation and the recoil phenomenon appear to be quite relevant. A working
phenomenological model would be important, of course, in order to optimise the effects and to
connect them to prior art. But the reported phenomena appear so new and peculiar that much
further experimental and theoretical work will probably be necessary for that purpose.

https://www.researchgate.net/figure/Scheme-of-device-by-C-Poher-CP-for-medium-voltage-discharges-in-a-superconducting_fig2_259106009

>>15647746
I don't get what any of this means

>>15647746
>>15647525
>>15647746
Epic /x/ thread meant for >>15647536

Thread got started because some anti-gravity researcher in Huntsville got DEW'd and killed herself due to chronic pain. Started out with a bunch of details about the case and then the whole thread turned into an anti-gravity physics paper brain dump.

There's a whole lot of these papers that depend on superconductors (macroscopic quantum states) for anti-gravity, gravitational wave communication, Mach effect inertial nullification and all kinds of crazy Star Trek shit. I'm not going to even pretend to understand most of it.

Don't know how real any of it is but the TL;DR seems to be that superconductors are (were?) the biggest hurdle to anti-gravity.

Oy vey shut it down!
We can't have Space CHUDs, they'll ruin the human livestock project
We need to keep everyone on the prison planet and consooming all the resources until the cattle are stuck here forever!

FWIW it seems LK-99 itself seems to be in a macroscopic state of whether it even works or not. Shrodinger's superconductor. Needs meme energy.

>>15647529
>>15647753
Fuck, why can't I figure out simple replies?
I picked the wrong week to quit sniffing glue.
The dumps above this are for you.

>>15646498
it's mild autism and overwhelmingly narcissism and other personality disorders. Many go into stem because they grew up doing nerd hobbies and they think extremely highly of themselves. Also these days they're preferentially hired.
>successful
Monetarily and status-wise yeah. Competence i'm pressing X on.

>>15647567
>>15647536
>>15647523
>>15647432
>>15647368
>>15647255
>>15647567
>>15647536
>>15647523
>>15647432
>>15647368
>>15647255
Are we ready to cook? Will be creating the thread shortly. See you all soon.

>>15648497
This will be the furnace we will be using, allow me the time to set up. I know it’s a mess. I have to clean my shit… I do it all the time but then after a couple of months this is what happens.

>>15648511
Forgot pic

>>15648515
While we wait, here is my 4 years old copper oxide.

>>15648521
Forgot pic again…

>>15648522
>>15648515
>>15648497
based and not cringe

>>15648533
I will be using exclusively shit I can gather from my surroundings.

For PbO - I will go to my local mechanic and ask him if I can have access to the discarded batteries. I know they have a ton. I will be scraping the positive electrode to extract any concentration of Pb0 that has formed. If anyone can, please confirm this for me.

PbSO4 - if anyone can advise on how to obtain this in a simple and efficient way I would appreciate.

Cu - I will use a harder metal to scrape a copper pipe and turn it into copper powder. I would like to make sure I avoid any contamination, if anyone has advice please let me know.

S - I can extract red phosphorus from match boxes strike strips. Can anyone advise wether it’s white phosphorus I need or if red phosphorus is fine?

>>15648554
The aim here is to make this process as simple and affordable as possible. To create instructions so easy anyone willing to replicate can have a clear guide to follow. Please contribute as this should be a team effort. The /sci/enfrens

>>15648571
To show that anyone can do this with just random shit they have laying around. And a furnace.

>>15648554
Sorry P not S.. bit distracted today sorry.

>>15647175
Use a tripcode and different temperatures in the process

>>15648620
What’s a tripcode?

>>15648632
Its a unique post ID so anons can indentify your posts
Use [Username]##[Password] in the “Name” section of your posts.

>>15648640
But its only used for AMAs and stuff
We call tripfags people that arent doing AMAs and are using tripcode

>>15648554
don't to this, it creates a room-temperature superconductor which is highly disruptive to the world economy

>>15648554
PbSO4 is the white stuff that collects on the plates of car batteries that have been sitting around too long. Probably comes with lead too. Pure lead sulfate can be made in a precipitation reaction with lead acetate. Get the lead acetate by boiling lead with distilled White vinegar and hydrogen peroxide, or react PbO with vinegar.

PbO is the most stable oxide around 600C. Heat up cushed car battery plates from new, charged battery, and slowly blow air through them. They are already very porous so this is the perfect source. Heat will drive off any sulfates, carbonates and organic matter.

If you end up needing sulfur to make the Cu2S impurity, it can be found in garden supply stores.

>>15648658
Thank you scienfren. Before we move on I would like to complete a simple guide to how to obtain each material necessary for the process. Following we will do the same for all the necessary equipment.

This is where we are now:

For PbO
>insert here

PbSO4 - can anyone confirm the following, I thought this was how you obtained PbO was I mixing up the two?
>is the white stuff that collects on the plates of car batteries that have been sitting around too long. go to local mechanic and ask him access to the discarded batteries in the name of science. Scrap the positive electrode to extract any concentration of PbS4 that has formed.

Cu - can anyone come up with a better way?
>Use a harder metal to scrape a copper pipe and turn it into copper powder.

P - white or red phosphorus?
> can extract red phosphorus from match boxes strike strips. Whet the stripe strip with a cloth, try not to let the cardboard soak. Scrape the red phosphorus into a small recipient, add acetone to melt any glue. Let it dry. This will give you small quantities but might be enough for what we need.

>>15648682
Here is the steps we will be taking

1. List of materials and how to obtain them
2. List of equipment and how to obtain it
3. Review together the South Korean methodology, set up three variants (including original) and begin testing.

Also, sorry for my shitty spelling. English is not my first language. I always notice my mistakes after I post. Forgive me for that.

>>15648682
You may be confused with the beige stuff that collects on car battery terminals (PbO), or the other oxide that can be found inside the battery (PbO2).

If red phosphorus is problematic then consider making the bulk of the material by reacting PbO with phosphoric acid, which is a cleaning supply and food additive. The CuO and whatever else can be added later. But this might not work because the copper doesn't bring any extra phosphorus to the table. This might be necessary for mixing on the atomic scale. Definitely best to try the given recipe first.

>>15648497
I'll be in when I can, I am at work atm

>>15648682
the quickest way to make relatively pure copper powder with very common materials while avoiding the annoying electroplating is chemically precipitating it out from solution
illustrative video guide: https://www.youtube.com/watch?v=dlHMYxZ99Gw
instructables guide: https://www.instructables.com/Make-Copper-Powder-From-Aluminum-Foil/

-1. you can just eyeball the measurements. just add an excess of aluminum foil then remove it once the reaction's done.

0. do not use iron/steel/cobalt/nickel tools that will be in contact with the copper sulfate crystals/copper powder. plastic spoons are recommended. for the hot parts, you could use a clean wooden stick - just anything that isn't a ferromagnetic metal

1. get some root killer (the blue copper sulfate crystals, CuSO4), dissolve it in DISTILLED water. you can try using hot/warm water to dissolve it faster

2. immerse aluminum foil (Al) in the blue solution.

3. add a pinch of table salt (NaCl) to start the precipitation reaction. the aluminum will dissolve, while the copper forms in the solution. THIS WILL GET HOT, so try wearing mittens or dilute the solution a bit with distilled water

4. the color should change from blue to cloudy brown. if it's still a bit blue, try adding a bit more aluminum foil and maybe a bit more table salt just in case.

1/2

>>15648682
>>15648828

5. let the solution cool down a bit (so you can hold it), then filter with a coffee filter. wash with boiling hot distilled water to remove as much impurities as you can (so the soluble aluminum sulfate gets washed out).
if you do not care about wastewater volume, you can use like a liter of hot boiling water to wash out any remaining impurities.

(if it were me, i would also wash it with pure hydrochloric acid (HCl) BUT commercial hydrochloric acid is usually contaminated with iron (which is why they're yellowish), so i would advise against this - unless you want to also purify hydrochloric acid too.)

6. if you're planning to store the copper powder for a decent amount of time, store it immersed in clean distilled water in a sealed closed container - this is to prevent the copper from oxidizing into copper oxide (CuO). if you have some dry inert gas around, you could store dry copper powder with it so you can avoid the hassle of having to evaporate away the water.

7. if you're planning to use it right away, dry the moist copper powder. you can do this by leaving it out for a day or drying it in somewhere warm (maybe like around 100°C max).

just make sure the powder doesn't turn black. the problem with drying copper powder is that the longer you leave it exposed to air and the higher the temperature is, the more it'll "rust" into black copper oxide.

if there's any errors in this post, i won't be able to correct it in time since i live in a way different timezone (UTC+8; basically asia timezone). if another chem anon is there, please do the needful sir

for amateur chemistry shit, sciencemadness is a good resource
https://www.sciencemadness.org/smwiki/index.php/Copper

i'm a bit concerned about contamination by aluminum, but i think this is the best we could do right away

2/2

>>15648554
Amazon sells large sheets of "match strike paper" for cheap

>>15648836
basic chemical reaction happening is this:
[math]2Al + 3CuSO_4 \rightarrow Al_2(SO_4)_3 + 3Cu[/math]
what's happening here is that you're dissolving the aluminum and replacing it with the copper part of the sulfate (SO4). the result is aluminum sulfate (Al2SO4) which is soluble in water (even more if boiling hot), and copper metal powder.

tl;dr try as best as you can dissolving away the impurities (aluminum sulfate, table salt, iodide, etc.) with hot distilled water.

btw just in case use a strong magnet to remove any traces of magnetic stuff in all your reagents.

>>15648682
enjoy synthesizing a low quality fridge magnet

I fucking hate tryhards. You aren't going to accomplish anything with some cheap equipment in your dirty garage.

>>15645066
Yeah and also they worked without gloves and superbacteria made it superconductor. And also one of a scientists opened door during creation in a perfect time which sent vibrations with a perfect amplitude.

>>15648911
I guess you're right, Chang. Thank you for looking out for our best interests by coming here and telling us how much you hate us.
China, Lockheed, prediction market speculators and big money stock buyers have no reason to poison the well.
We should stop wasting time with this and go back to videogames and hentai.
I'm feeling sleepy.

>>15648865
>>15648836
>>15648828
Thanks for your effort posts.

If some anon here manage to actually recreate some of the LK-99 with some semblance of accuracy, you guys can finally join the other boards that actually manage to get shit done.

>>15648828
>>15648836
>>15648865
Thank you for helping. Here is the updated list of materials and how to obtain them.

For PbO
>insert here

PbSO4 - can anyone confirm the following, I thought this was how you obtained PbO was I mixing up the two?
>is the white stuff that collects on the plates of car batteries that have been sitting around too long. go to local mechanic and ask him access to the discarded batteries in the name of science. Scrap the positive electrode to extract any concentration of PbS4 that has formed.

Cu - you will need: copper sulfate, aluminum foil, h2o, and salt
Here is a tutorial: www.youtube.com%2Fwatch%3Fv%3DdlHMYxZ99Gw
>the quickest way to make relatively pure copper powder with very common materials while avoiding the annoying electroplating is chemically precipitating it out from solution.

P - you will need: match boxes, acetone, cotton, water, a small spatula
Here is a tutorial: https://youtu.be/5ZrfNAHDjWU
White or red phosphorus?
> can extract red phosphorus from match boxes strike strips. Whet the stripe strip with a cloth, try not to let the cardboard soak. Scrape the red phosphorus into a small recipient, add acetone to melt any glue or impurities. Let it dry. This will give you small quantities but might be enough for what we need.

>>15648515
>>15648522
>>15648554
Wishing you luck anon. Godspeed

>>15649022
>PbSO4 - can anyone confirm the following, I thought this was how you obtained PbO was I mixing up the two?
Kind of a mix of both. The way that those work has the battery acid (which is just sulfuric) reacting with lead oxide to produce lead sulfate, which later reverts to the oxide and acid.
The stuff that tends to gather is lead sulfate that doesn't revert, but a bit of lead oxide might be present.
In either case, you can chuck the shit into some concentrated sulfuric to get the sulfate for certain, and you can make the oxide from the sulfate rather easily by just mixing it with some lye or whatever other hydroxide (and heating it to ~135 degrees Celsius on the off-chance that you've somehow stumbled on a way to make lead(II) hydroxide).
>White or red phosphorus?
Red. Red, red, red, red, red. White phosphorus will fuck you up. Nobody in their right mind is working with it unless absolutely necessary.

>overspammer fags:
>asian papers that replicate some of the korean results: LE CHINK SHIT
>asian papers that don't replicate the results (and didn't follow instructions): ITS LE OVER!!1

>NO DON'T BOTHER TRYING TO DO IT YOURSELF REEEEEEEEE
why are overfags like this? Im not even a backfag I just want to see what happens. Is it because of the stupid fucking gambling people are doing?

>>15649118
nobody replicated the Korean paper results retard

>>15649118
mental problems. some people are so weird and spiteful that they actually dont want this to be real and anything you might do that indicates you think its real enrages them.

>>15649124
>chinese aren't people
hello /pol/

>>15649133
no Chinese lab replicated the Korean paper results

>>15649118
17 century scientists did real sciene without a california degree from MIT.

lmao at the current state of basedciense.

>>15649118
>Is it because of the stupid fucking gambling people are doing?
Mostly, yes. The prediction markets brought over a horde of /biz/tards. There are also a few Pajeets trying to save face for that abysmal Indian replication attempt.

>>15646498
Wishful thinking. Trannies are terrible programmers

Are we happy with this, If so let’s move on to equipment. Let me know.

PbO - if there is a better way please update the following.
you will need: lead nitrare, a stainless steel crucible, a blow torch
Here is a tutorial: https://youtu.be/KeDV3zmowwM

PbSO4 - you will need: old car batteries
>is the white stuff that collects on the plates of car batteries that have been sitting around too long. go to local mechanic and ask him access to the discarded batteries. Scrape the positive electrode to extract any concentration of PbS4 that has formed.

Cu - you will need: copper sulfate, aluminum foil, h2o, and salt
Here is a tutorial: https://youtu.be/dlHMYxZ99Gw
>the quickest way to make relatively pure copper powder with very common materials while avoiding the annoying electroplating is chemically precipitating it out from solution.

P - you will need: match boxes, acetone, cotton, water, a small spatula
Here is a tutorial: https://youtu.be/5ZrfNAHDjWU [Open]
White or red phosphorus?
> can extract red phosphorus from match boxes striker strips. Wet the red striker strip with some cotton, try not to let the cardboard soak. Scrape the red phosphorus into a small recipient, add acetone to melt any glue or impurities. Let it dry. This will give you small quantities but might be enough for what we need.

>>15649287
probably want to do this outside and with a respirator

>>15649290
Yes thank you. Let me add that as a general warning for working with lead.

>>15646421
Based. Really fortunate to have found the Fuhrer to lead me through this chaos.

>>15649287
How to make lead nitrate: https://youtu.be/ZYNEHwHAtqk

>>15648554
Good luck anon and be safe! Gloves, safety glasses and all that. Especially when working with acid car batteries. But it sounds like you know what you're getting into. You brought back my hype

if someone can review what we have till now and make sure we did not forget or skip anything. Also, I want to make sure the following point is correct. Thanks
PbSO4 - you will need: old car batteries
>is the white stuff that collects on the plates of car batteries that have been sitting around too long. go to local mechanic and ask him access to the discarded batteries. Scrape the positive electrode to extract any concentration of PbS4 that has formed.

>>15647746
>>15647761
>/x/
Fuck off and die.

>>15649369
you wont allow information in based on arbitrary
limits you made of some inane emotion

Updating again:

Please remember. When working with lead and stuff: always be in a well ventilated space, wear gloves, wear mask, do not inhale smokes

PbO - if there is a better way please update the following.
you will need: lead nitrare (tutorial for lead nitrate: https://youtu.be/ZYNEHwHAtqk)) , a stainless steel crucible, a blow torch
Here is a tutorial: https://youtu.be/KeDV3zmowwM [Open]

PbSO4 - need to confirm this is a viable method, if not please propose alternative.
You will need: old car batteries
>is the white stuff that collects on the plates of car batteries that have been sitting around too long. go to local mechanic and ask him access to the discarded batteries. Scrape the positive electrode to extract any concentration of PbS4 that has formed.

Cu - you will need: copper sulfate, aluminum foil, h2o, and salt
Here is a tutorial: https://youtu.be/dlHMYxZ99Gw [Open]
>the quickest way to make relatively pure copper powder with very common materials while avoiding the annoying electroplating is chemically precipitating it out from solution.

P - you will need: match boxes, acetone, cotton, water, a small spatula
Here is a tutorial: https://youtu.be/5ZrfNAHDjWU [Open] [Open]
> can extract red phosphorus from match boxes striker strips. Wet the red striker strip with some cotton, try not to let the cardboard soak. Scrape the red phosphorus into a small recipient, add acetone to melt any glue or impurities. Let it dry. This will give you small quantities but might be enough for what we need.

>>15647203
Aw, someone's angry.

MUSTARD GAS

>4chan retards will make leading edge science on their garages that western universities wont do

>>15649410
For me this started because I am sick of hearing people repeating whatever they read on their news without having any idea what they are fucking talking about. I’m sick of institutions telling us something is not possible and provide a bullshit excuse to shut it down and kill all hope, enthusiasm and discourage further attempts. I’m sick of payed sluts selling off humanity for whatever benefit they can get. Creating this RTSC happens to be something everyone can do. So rather than having someone telling me it’s fake I will do it my self and verify it, if frens shan’t to join than this will better our odds of success. You can keep trusting your experts to do the work for you. Don’t you dare try something yourself and maybe end up learning something new along the way.

>>15649410
>>15649401
>>15649188
>>15649128
Pic related.

We don't need anyone's permission to do it, we don't need to go through ten fucking committees, we don't need to write a grant proposal, we don't need to beg the government for gibs at all, we don't need to fill out HASEPs, we don't need to find the right mix of diversity hires to put on the paper, we don't need to do 10 dense pages of x-ray diffraction and density functional calculations, and we don't have a reputation to risk.

Just make it, see if it floats, play with it if it actually does. No resistivity measurements even required in that case. Just videos that would be hard to fake.

Imagine the seethe if it actually works!

>>15649435
This. Posted before I saw yours, but so much this.

>>15649380
Do the boat test. Make them seethe even more for not thinking of it.

>>15649447
enjoy dying in your garage when you vaporize the lead and end up breathing it

>>15649617
Would you gloat over my death? Would a bunch of science soibois taptance on the grave of the dumb redneck who didn't Trust The Experts? This is starting to remind me of Covid. We will know for sure if red phosphorus gets the horse paste treatment.

>>15649128 is right about you. You're a spiteful mutant NPC. You fly into a jealous rage when confronted with the fact that some people have qualities you don't, namely rugged individualism, creativity and Faustian spirit.

>>15649447
The issue with "basement replication" attempts is that while successes can be counted, failures can't.
Even then, successes aren't necessarily conclusive as you could have a contaminated sample, like iron filings from a hammer.
Doing it yourself is fine, trying to use that as evidence of something being real/fake isn't, as you have no proof of your rigor.

>>15649673
Just a pro tip. If you live in the US, and also generally in modern techno dystopia hell hole, you probably shouldn't go look up sources for red phosphorous if you don't want to be bothered by letter soup agencies of different variety..

>>15649684
Aren't matchheads a good choice?

>>15647746
It's obvious this is a scam to get tons of inverstors money. She faked her own death and is now enjoying her billions of USD.

>>15649837
To make LK-99? Yeah sure if you want to scrape 10298384738 of them. And if you want a heavily contaminated low quality batch, also...

So let me get this straight
>you won't accomplish anything
>might kill yourself
>get in trouble with the law
>costs lots of $
>takes forever
and you still want to try?

>>costs lots of $
not even ligma balldrich could figure out a way to jack up the prices beyond a few hundred dollars for everything you'd need
and it's not that long of a reaction, either, though I guess if you're a tourist you don't know what a long reaction is

>>15649867
would cost a lot of $ if you wanted to make a meaningful attempt. a proper furnace alone is at least $8000

or you could just go with the classic blowtorch and propane tank for under $100
sure, you're not producing fifty kilos of the stuff that way

>>15649884
you can't use a blowtorch for 76 hours!
it's completely unrealistic to even attempt making it in your basement

>>15649844
You get the red phosphorus from the striker strip not the match head.
>>15649862
>you won't accomplish anything
Even if I don’t, I will still learn from the experience
>might kill yourself
Use fear that trick always works. Ma mustard gas. Just take the right precautions and understand what you are doing and what are the reactions. Never follow blindly
>get in trouble with the law
If you are a murican
>costs lots of $
No, can be done with everyday stuff, except the furnace that you can get for $500
>takes forever
If you attention span is a 10 sec tiktok video

>>15649684
Yeah I'm not even going to try to buy anything that can't be found in the grocery store or Home Depot. If I even make it at all, which realistically I probably won't, and if I did, I wouldn't begin the process for at least two weeks. I've just been looking up a bunch of chemicals on Wikipedia. If anyone digs deeper into my internet history it will lead them here and to text messages with a friend who has been asking about this stuff for a sci-fi / fantasy book.

>>15649682
Videos can be a lot better. See >>15649450
The point is to remove the gatekeepers' monopoly on "It's over" and get other people to start making it, start trying different methods etc, because the current method gives such widely varying results that I think it's non-deterministic so there are going to be a lot of failures anyway. Let those failures stay in peoples' basements. It's better than not attempting at all. The few successful methods will bubble up, mutate and evolve, until results become undeniable.

>>15649844
Yeah the phosphorus is probably going to be the main problem.
What about dissolving magnesium in phosphoric acid, drying it, throwing in some aluminum powder, heating it up without oxygen. Give the oxygen something it wants to attach to more than phosphorus. Just spitballing here. There are three kinds of magnesium phosphate and I have no idea what the mix would be, what temperatures would be involved, what safety precautions to take. A similar idea might work with bone meal or phosphate fertilizer but there would be a lot of contamination of the sample.

Could try to make the bulk material with PbO + phosphoric acid and mix in CuO and maybe Cu2S later, but then the Cu doesn't bring any phosphorus to the table so it might not get thoroughly mixed into the material. IDK

>>15649871
A pottery kiln might do it. $1000 or less.

>>15649895
>Come back every few hours and swap the propane tank
Not difficult.

>>15649905
this is insane. criminals will start using LK-99 as a excuse for their meth labs

>>15649905
I payed this kiln 1000 euro, it meets all the requirements. And you could even get a smaller one now days for less.
>>15648515
>>15648497

>>15649912
Governments are going to start using meth labs as an excuse to lock up basement-dwelling LK-99 alchemists

>>15649862
What sort of personality defect do you have to have to think like this? People like him are who drive the world, while people like you only fill an ancillary role to his existence.

>>15645303
yes

Hi frens. I made a new thread. Please come join!

>>15651224
>>15651224
>>15651224

>>15649912
Ok? we shouldn't be banning base materials because they can be misused, that is like banning lathes because they can be used to make unregistered guns.

>>15646498
Yeah, in the same way that being a deer is correlated with getting stuck in deer traps. Autists naturally become programmers and scientists. They're groomed into this cult and get fried out on hormones instead. See >>15649200; a young autistic man gets a few years of being a successful trans programmer before the estrogen fries his shit.

>>15649410
This shit is optimized for existing coders, free to use in a web browser and if it ever paywalls (unlikely) some random autist will just replicate it in a FOSS VSCode extension or something. It's gonna be insane. Plasmid trade and manufacture is barely regulated at all and the Chinese don't care anyway; in-garage gene science is gonna push biology/biochem forward the way garage startups 10x'd computers.

Some anon is gonna fucking cure cancer and post it anonymously to GitHub with a Touhou avi.

>>15651774
Don't forget everyone and their mother having access to:

1. AlphaFold, which allows for infinite simulated protein manufacture without needing to do it in the lab (enabling a run-debug cycle for gene editing)
2. LLM's (hopefully open source ones, too!) trained specifically on gene sequences that will basically act as a kind of GitHub copilot for bedroom gene editors.

BenchLing already implements #1 and is working on #2. Imagine John Carmack working on the human genome. Shit's gonna be nuts.

>>15645506
>the koreans may have lied through their teeth, but the chinese NEVER would

>>15649188
>scientists, 1750: "NULLIUS IN VERBA; I'm gonna go home and replicate your experiment right the fuck now"
>scientists, 2023: "NOOOOOO YOU DIDN'T DO A HECKIN' PEER REVIEW YOU CAN'T JUST PUT SHIT ON ARXIV AND LIVESTREAM YOUR EXPERIMENTS WHERE IS YOUR ETHICS IMPACT STATEMENT GET BACK HERE"

PbO
>warning:
Lead salts are highly toxic. Nitrogen dioxide is highly toxic. Safety precautions must be in place to protect yourself, especially from the NO2.
>tutorial:
- https://youtu.be/KeDV3zmowwM
>you will need:
- Precision scale
- lead nitrare (tutorial for lead nitrate: https://youtu.be/ZYNEHwHAtqk))
- 1 stainless steel crucible
- blow torch
- aluminum foil


PbSO4
>warning:
- Lead compounds are highly toxic. Safety precautions must be in place to protect yourself.
>you will need:
- old car batteries
>description
is the white stuff that collects on the plates of car batteries that have been sitting around too long. go to local mechanic and ask him access to the discarded batteries. Scrape the positive electrode to extract any concentration of PbS4 that has formed.
>Alternatively method tutorial:
- https://youtu.be/bnbxYPMBz9M


Cu
>warning:
- Copper sulfate is toxic. Do not eat, drink or touch. Safety precautions must be in place to protect yourself.
>tutorial:
- https://youtu.be/dlHMYxZ99Gw
>you will need:
- copper sulfate (can be bought in store as root killer)
- aluminum foil
- h2o
- salt
- precision scale
>description:
the quickest way to make relatively pure copper powder with very common materials while avoiding the annoying electroplating is chemically precipitating it out from solution.

P
>warning:
Red phosphorus is a controlled substance in certain countries
>tutorial:
https://youtu.be/5ZrfNAHDjWU
>you will need:
- match boxes
- acetone
- cotton
- water
- a small spatula
>description:
can extract red phosphorus from match boxes striker strips. Wet the red striker strip with some cotton, try not to let the cardboard soak. Scrape the red phosphorus into a small recipient, add acetone to melt any glue or impurities. Let it dry. This will give you small quantities but might be enough for what we need.

>>15652456
STEP 1: Preparation for lanarkite - Pb2SO
>you will need
- Agate mortar with a pestle
- Aluminum crucible
- Furnace
>process:
PbO and PbSO4 powders were uniformly mixed in a molar ratio of 1:1 in an agate mortar with a pestle. And then, after the sample was transferred to an alumina crucible, it was reacted at 725 °C for 24 hour in a furnace. After completion of the reaction, white sample was obtained. It was pulverized with the mortar.

STEP 2: Preparation for copper phosphide - Cu3P
>you will need
- Quartz tube
- Furnace
>process:
Cu and P powders were mixed in each composition ratio. And the sample was transferred in a quartz tube. The tube was sealed and reacted at 550 °C for 48 hour in a furnace. After taken out from the tube, a dark gray ingot was obtained and pulverized.

STEP 3: Sample Synthesis and Preparation of LK-99
>you will need
- Agate mortar with a pestle
- Reaction tube
- Furnace
>process:
For the sample synthesis of the LK-99, the general solid-state reaction was used. Lanarkite and Cu3P were uniformly mixed in a molar ratio of 1:1 in an agate mortar with a pestle. The sample was put into a reaction tube and reacted at 925°C for 10 hr. After the reaction, a dark gray ingot was obtained reproducibly and then made into the shape of thin cuboids for electrical measurements. For other analyses, it was pulverized and used as the form of powder. The reagents used for the above solid- state reaction was PbO (JUNSEI, GR), PbSO4 (KANTO, GR), Cu (DAEJUNG, EP), and P (JUNSEI, EP).

>>15651782
AlphaFold does not help in designing proteins
>.t knower

>>15649905
>The few successful methods will bubble up, mutate and evolve, until results become undeniable.
The problem is that we have had a good number of replications with formal institutions trying not to mention amateur results and none of them have definitive proof showing ALL of the claimed properties in the original paper written by the gooks. People have shown bits and pieces but not checklisting every point in the original paper. By all means, no one is stopping anyone from trying it, the synthesis method is public but convincing anyone else without even actually having the said material with ALL of its properties as a superconductor has yet to be done. We wouldn't be having the discussion about it possibly being a fraud otherwise if the gooks actually had a reliable synthesis method or if multiple people managed to actually measure everything the paper claimed.

>>15647487
>cut them with 90 degree angles
A string with a weight to get the 90 degree angles
> without power tools
Guess what? People in the Middle Age didn't have power tools too. And even today, it's not uncommon for stonecutters to not use such tools. (t. I work as a stonecutter for some time.)
>the rocks look like they were soft and then were hardened in place
Erosion

https://arxiv.org/abs/2308.04353

>>15652675
Over? Back?

AirChads, what makes us so much better than vacuum incels?

>>15652687
It's nothing new. The same "whatever this is, it can't possibly be superconducting" Chinese discredit paper that got churned out over the weekend.

>>15652687
>>15652687
Change in resistance caused by first order transition of Cu2S at around 400k was misinterpreted as superconductivity. From the Institue of Physics of the Chinese Academy of Sciences.

>>15652688
Presence of oxygen

>>15652708
https://scholar.google.com/citations?user=ofG2kjUAAAAJ&hl=en
https://www_facebook_com/100008122782686/videos/661722942350287/

>>15652708
this

do any of you niggers even remotely understand what is going on at all?

>>15652968
Who said that?? Where the fuck am I? This isn't the post office!

>>15646539

>>15645209
it was shot with a ray of my omega beams that transfixed it

>>15653172
It's so over

>>15653172
imagine thinking this psychotic tranny is trustworthy for anything regarding their lk99 claims, much less anything else

>>15649895
There's nothing stopping you from just going to the store and buying more propane..

>>15653193
The fact that McCalip took them seriously doesn't inspire confidence in him either.

>>15652704
What about all the other odd properties?

>>15653172
common iris W

>>15653208
point well taken...

>>15649673
Based image.

>>15653172
>not following

>>15645299
>t. biolonigger

>>15653172
I honestly wish that faggot gets sent to Bakhmut.

>>15654323
Isn't that a summon from final fantasy?

I don't wanna play this game no more

>>15653208
I think the same. "Iris" allegedly did show some level of knowledge but really, a little bit of conservative caution won't hurt you.

>>15645209
based Super Mario 64 reference