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>> No.12265330 [View]
File: 146 KB, 1280x720, fatty acid ester synthesis.png [View same] [iqdb] [saucenao] [google]
12265330

>>12258748
It sounds like you aren't actually forming your Gilman reagent. Have you tried to form your alkyl lithium just from the alkyl halide and lithium metal?

Also a quick search of Sci-finder has very few examples but they usually form a Grignard first.

Going off this paper: Huber et al. J. Organomet. Chem. 2013, 744, 144-148. see pic related.

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